The MS17AM is a manual valve version of the MS17AB. Since it is a manual
unit, some care must be exercised in the sequencing of the valves. The
most important things to remember are that during normal leak testing:
1. The THROTTLE VALVE is NEVER opened unless the ROUGH VALVE has been operated first. In cases of large leaks, the ROUGH VALVE may still be open while opening the THROTTLE VALVE.
2. The THROTTLE VALVE is ALWAYS closed BEFORE opening the VENT VALVE. The only exception is during servicing.
3. The VENT VALVE is NEVER opened if either the THROTTLE VALVE or the
ROUGH VALVE is open. Again, the exception is during servicing.
MS17AM OPERATING INSTRUCTIONSWARNING
These instructions are not to be used for the MS17AB or MS17ABC. Instructions
for these units will be found in the manual.
I. Starting from a total shut down.
a. Position of Valves and Control Switches
Rough Pump.Off Rough Valve.Open
Forepump..Off Throttle Valve...Closed
Diffusion Pump.Off Test portCapped or connected to test object
Electronics.Off
b. Procedure
1) Plug the power cable into a 115 volt, 60 Hz source.
2) Plug the cord of the REMOTE LEAK METER into the socket on the rear,
upper left part of the unit housing.
3) Cap the TEST PORT, or, connect to the test object.
4) Turn on the FOREPUMP switch. A gurgling sound will be heard, caused by the high pressure air being exhausted from the pump.
5) With THROTTLE VALVE open and ROUGH VALVE closed, the forepump can be monitored on the MANIFOLD PRESSURE meter (the thermocouple for the manifold meter is between these two valves, see diagram). Pressure should not exceed 500 millitorr. Once the pressure holds at 500 millitorr or less, close the THROTTLE VALVE and turn on DIFFUSION PUMP. The FOREPUMP and DIFFUSION PUMP switches are interlocked so that the diffusion pump cannot operate unless the forepump is on. You will not be able to monitor the pressure obtained by the diffusion pump until the electronics are turned on later.
6) Turn on the ROUGH PUMP and open the ROUGH VALVE. The pressure obtained by the rough pump will be displayed on the MANIFOLD PRESSURE meter.
7) After about 20 minutes (time needed for diffusion pump to heat up),
turn on the ELECTRONICS switch. Turning on the electronics too soon can
contaminate certain components. Monitor the pressure on the HI-VAC PRESSURE
meter. If the pressure reading is off-scale, shut off the ELECTRONICS switch
and wait a few more minutes. It can take a longer time to pump down if
there is condensation in the cavity surrounding the cold trap.
WARNING Never obstruct the filler opening of the cold trap fill pipe as pressure builds up due to nitrogen evaporation. Always wear protective gloves and eye protection when working with liquid nitrogen.
8) When the HI-VAC PRESSURE reads 10-4 Torr or lower, add liquid nitrogen (LN2) to the cold trap. Start by adding a small amount to the trap and wait. After about 3 minutes fill the trap the rest of the way. The HI-VAC PRESSURE should drop to 5X10-5 Torr or lower in a few minutes.
9) Push the FILAMENT switch to on. This should light the EMISSION lamp
on the front panel and the TEST lamp on the remote meter. These lamps should
remain lit. If the HI-VAC PRESSURE gets higher than about 3X10-4
the
filament will automatically turn off. If this happens you should:
a. check the cap on the test port, or, if you are connected to the test object, check connections.
b. evaluate if your leak is large enough to detect by other means.
II. Leak Testing - Typical
a. Procedure
1) If not already done, connect the object to be tested to the TEST PORT. Tighten the quick coupling securely. The electronics must be on and the cold trap filled.
2) Open the ROUGH VALVE fully and
pump down to 20 millitorr. If 20 millitorr cannot be reached, see Section
III.
3) Close the ROUGH VALVE and slowly
open
the THROTTLE VALVE fully. The HI-VAC PRESSURE meter should read less than
2X10-4 . Turn the FILAMENT on. The EMISSION lamp should stay
lit.
4) Set the Volume and Scale on the REMOTE LEAK METER so that a low, steady tone is heard.
5) Spray the test object with helium, watch for the needle to deflect and listen for the tone to get higher in pitch. There can be a delay of as much as 10 seconds between helium spray and detection by the Mass Spectrometer, be patient.
6) When the leak test is done, close
both the THROTTLE and ROUGH VALVES. Open
the VENT VALVE until the test object is fully vented to atmosphere. Disconnect
the test object and close the VENT
VALVE.
III. Leak Testing Large Leaks, Large Gassy Volumes
Occassionally, the manifold pressure will not go down to 20 millitorr.
This is either due to a large leak, several small leaks, or a very large
volume that is slow to pump down. In these cases a slightly different technique
is used in operating the valves.
a. Procedure
1) If not already done, connect the object to be tested to the TEST PORT. Tighten the quick coupling securely. The electronics must be on and the cold trap filled.
2) Open the ROUGH VALVE fully and
pump as low as possible. If pressure is above 20 millitorr it must be "throttled"
into the high vacuum section.
3) Slowly open the THROTTLE VALVE
until a reading of between 5X10-5 and 1X10-4 is read
on the HI-VAC PRESSURE meter. Note that the ROUGH VALVE is still open.
4) Spray the test object with helium and monitor the REMOTE LEAK METER.
Use a minimum of helium at first because there may be a large leak. Increase
the helium dose if nothing is detected.
5) When the leak test is done, close
both the THROTTLE and ROUGH VALVES. Open
the VENT VALVE until the test object is fully vented to atmosphere. Disconnect
the test object and close the VENT
VALVE.
IV. Partial Shut Down (Overnight or Weekend)
a. Procedure
1) Cap the TEST PORT. Tighten the quick coupling securely.
2) Open the ROUGH VALVE until 20
millitorr or less is reached.
3) Close the ROUGH VALVE. The THROTTLE
and VENT VALVES should already closed.
4) Turn off the ELECTRONICS.
V. Complete Shut Down
a. Preparation
1) The cold trap must be at room temperature before a complete shutdown
can be performed. Leave the unit in the "Partial Shut Down" configuration
until the LN2 evaporates and the cold trap warms to room temperature.
Leave a note on the unit saying that it is warming up for a complete shut
down. This is to prevent condensation from forming in the vacuum chamber
around the cold trap.
b. Procedure
1) Turn off the ELECTRONICS.
2) Turn off the DIFFUSION PUMP. Note the time.
3) Wait 30 minutes after turning off the diffusion pump.
4) Verify that the COLD TRAP is at room temperature. If not, wait until
it is.
5) Open the ROUGH and THROTTLE VALVES
and pump down to 500 millitorr. Close
the THROTTLE VALVE. Turn off the ROUGH PUMP. Open
the VENT VALVE until pressure equalizes. Close
the ROUGH VALVE.
6) If it has been at least 30 minutes since step (3), open the THROTTLE VALVE. Turn off FOREPUMP. Close the VENT VALVE.